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UNK07.TXT
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1993-02-12
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5KB
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205 lines
Insoluble in the usual reagents.
1348
The unknown is neither acidic nor basic.
Solvent is deuterochloroform.
ß▀▄╓╨╪╪▌ßπΓ▌█╒╦╠╧╧╓ασσµµµµµµµµµµµµµτµµµµσσµτµµµµµττµσΣΓ┌╤└╤αΓΣπΓα┘╥═╙█Σσµττττµτττττµµσσσµµµµµµµµµµµµµµττττττττττττµττττττττττττττττττττττττττττττττµτµµτττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττττµµµµµµµµµµµµµµµµµµµµµµµµµµµ
µττττττττµµττττττττττττττττττττµµττττττττττττττττττµµτττττττµµµµµµµµµµµµµµµµµµµµσσµµµµµµµµµµµµµττττττττττττττττττττττττττττττττττττττµµµµµµµµσσσσσΣΣπΓα▐▄┘╗▓) Dï╢╥ßπΣΣσσσσπΓπσσσσµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµµτττττµµµµµµµµµµµµµµµµµµµτττ
τττµµµµµµµµµµµµµµµΦΦΦΦΦΦΦΦΦττττττττττττττττµµµµµµµµµΦΦΦΦΦΦΦΦΦΦΦττττττττµµµµµµµµµµµµµµτττµµτττµµµσπΓ┌▄╒╤╓ΓσµτΦΦΦττΦΦΦ"╩!4╩!T!¿ #
ΦΦΦΦΦΦΦΦΦττττττττττττττΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦΦτττττττττττττττττττττττττττττττττττττττττττµµµµµµµτττττµµττττττττττττττττττµµτττΦΦΦΦΦττττττττΦΦΦΦτττττττττττµσΣα▄╙└└┐╛═╓ΣσσσσσσσσσσσΣΣL
132023303334383941424344454648495154
There is a ratio of 3 aromatic H's (1,2,4-trisubstituted ?) to 1 methyl group.
#
dummy ms
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Only nitrogen was detected.
264048
Could be an amine, amide, cyanide, nitro compound etc.
Burnt with a smoky flame leaving no residue.
#
Behaviour typical of an aromatic compound.
70 to 73 degrees.
#
A low melting solid.
Nujol mull.
##!"!""$""#$$#$%%$%$#$$$$$$###$$%&%&&%%%&&&&'&&'''''((((('((((''(((()())()(*,,,,,,-/2=KyreYQTKJLR`é£╔╔╓Γ┌─╡⌐₧Ñ╕ªycE84/,+)*-//-,,,,-,,++,-+**)***)))*++++********)()(())**)((((((''''''&'&&&&'''&&&&&&&%%%&()+(&&$$$$$$$$$$$$$$#$%&&()+*(&%$#####$$$##"""""#$$$%
&&$$$""#$&,/=gö╖Åq]UMHBCJió═▄µΦσß┌╦║¥ëévlnzïæùÅ{riYI>765AMOuï⌐╖╦╓ßσ═╚ñÅ|nkg`WSOJQgYLDA><:989:?J>966521SY^^<?H<53..//0.0O`MC<633?B2-+++)((*+*((((())/L~âW8+*('%%+''/On~G4*&&$&cU;/,3A5..9{¥jH;BcbB+'%(23(#"!4IA,&$$##$###""##" "',-,(%#$%*9A3($ ""$&&)*(1.
131419202223242728293033343839414243444546484950515354
The compound is aromatic; absent are C=O, N-H, O-H bonds.
The compound decomposed before distilling.
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Typical of many organic solids.
Optically inactive.
#
The unknown is not chiral.
Not usually measured for a solid.
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Best to do this measurement on a liquid.
Not usually measured for a solid.
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Values are not readily available for solids.
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No reaction was seen.
2227282950
This unknown is not a ketone nor an aldehyde.
No reaction at room temperature.
3344454651
The unknown is not an alcohol, acid or phenol.
No positive result could be obtained.
#
The compound is not an amine.
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No change in colour was seen.
14
The compound is not an ester.
A silver mirror was formed.
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The unknown contains one or more nitro groups.
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No reaction was observed.
3344454651
The compound is not an alcohol, phenol or prim. or sec. amine.
A negative result.
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Unknown 7 is not an amide.
No reaction at room temperature.
#
The unknown is not unsaturated or easily oxidised.
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No change was obseved.
232850
The unknown is not a sugar.
A brown precipitate formed in a short time.
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This unknown compound has one or more nitro groups.
No change was observed.
#
The compound is not a phenol nor is it unsaturated.
No positive result.
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Ether groups are absent.
No colour change was seen.
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The unknown is not a phenol.
No change in colour noted.
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The unknown is not a primary amine.
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No reaction took place.
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Absent from the compound are primary or secondary amino groups.
No positive result.
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The unknown is not an amino acid.
No nasty smell formed (hurrah).
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The compound is not a primary amine.
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Very vigorous reaction.
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Typical of most oxygen and nitrogen containing compounds.
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No positive result.
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The compound is not a primary amine.
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No reaction took place.
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The compound is not a phenol nor unsaturated.
No change was observed.
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Absent are groups like esters, amides, cyanides etc.
No reaction was observed.
3344454651
The compound is not an alcohol, primary amine or secondary amine.
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pale yellow crystalline solid
01050725
0
818795
Colourless crystals m.p. 180-183 degrees.
Solid with m.p. of 97-100 degrees.
Yellow crystals m.p. 79-82 degrees.
2
ê£Ü¥ñ▒n⌐╞oô╛½¡╞╖k¬
ç¥│╡┤░y¼ƒOp₧ëÑ║└f╣╗iûÑ┐─ó╖¿
solid nitro compound
4
2,4-dinitrotoluene
1-methyl-4-nitronaphthalene
3,5-dimethyl-1-nitrobenzene
4,5-dimethyl-1,3-dinitrobenzene